Extended knowledge of 5-Bromoisoindoline-1,3-dione

According to the analysis of related databases, 6941-75-9, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6941-75-9, name is 5-Bromoisoindoline-1,3-dione, This compound has unique chemical properties. The synthetic route is as follows., SDS of cas: 6941-75-9

Synthetic Example 3; Synthesis of 4-bromophthalamide (hereinafter abbreviated as 4-BPA); [Show Image] 4-BPA represented by the formula (21) was synthesized from 4-bromophthalimide (hereinafter abbreviated as 4-BPI) according to the following procedure (reaction formula 3) with reference to Journal of Heterocyclic Chemistry, 1995, pp. 495-498. In a 100-ml eggplant flask, 27.8017 g (0.123 mols) of 4-BPI and 60 ml of 20% ammonia water were placed followed by reaction under stirring at 23C for 48 hours. After completion of the reaction, the reaction solution in the form of a white suspension was allowed to stand at 0C for one hour, followed by filtration under reduced pressure. The resulting white solid was dried in a reduced pressure dryer at 23C or 24 hours to obtain 29.90 g (yield: 75%) of a white powder of 4-BPA. The thus obtained white powder was subjected to identification of the structure thereof from NMR spectra and confirmed as 4-BPA. 1H-NMR (ppm/DMSO-d6):delta 7.84(s, 1H), 7.78(s, 1H), 7.67(d, 1H), 7.65(d, 1H), 7.62(d, 1H), 7.43(s, 1H), 7.40(s, 1H).

According to the analysis of related databases, 6941-75-9, the application of this compound in the production field has become more and more popular.