In chemical reaction engineering, simulations are useful for investigating and optimizing a particular reaction process or system., Product Details of 25369-33-9
To a coo?ed (0 C) soution of 7-choroindohn-2-one (1 g, 6.0 mmo) in TFA (11 mL) was added Nbromosuccinimide (1 g, 6.0 mmo) portion wise and stirred the mixture at same temperature for 6 h. Concentrated TFA in vacuo with DCM (25 mL) and then with EtOAc. The crude product was triturated with ethano to provide the tiDe compound as a white soid (861 mg, 58% yie?d). MS (ES):mass cacd, for C6H5BrCNO, 244.9; m/z found, 246.0 [M+H]. 1H NMR (500 MHz, DMSO d6) oe 10.92 (5, 1 H), 7.52 7.48 (m, I H), 7.38 (d, J = 1.2 Hz, I H), 3.62 (s, 2H).
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Reference:
Patent; JANSSEN PHARMACEUTICA NV; AMERIKS, Michael K.; RAVULA, Suchitra; SAVALL, Bradley M.; SWANSON, Devin M.; ZIFF, Jeannie M.; SHIREMAN, Brock T.; (167 pag.)WO2016/176463; (2016); A1;,
Indoline – Wikipedia,
Indoline | C8H9N – PubChem