Recommanded Product: 366453-22-7,Chemistry involves the study of all things chemical – chemical processes, chemical compositions and chemical manipulation – in order to better understand the way in which materials are structured, how they change and how they react in certain situations.
Step c: To an ice-cold solution of [11C] (291 mg, 1.78 [MMOL)] in CH2CI2 (20 mL) was added a 1.0 M BBr3 solution in [CH2CI2] (3.6 mL, 3.6 [MMOL).] The cold bath was then removed and the resulting solution was stirred for 16 h at ambient temperature. The reaction was carefully quenched by the addition of water and the mixture was extracted with EtOAc. The combined extracts were washed with water and brine, dried [(MGS04),] filtered and evaporated to dryness to give [11D] (232 mg, 87% yield) as beige solid.
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Reference:
Patent; BOEHRINGER INGELHEIM (CANADA) LTD.; WO2004/26875; (2004); A1;,
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