9/3/2021 News Research on new synthetic routes about 16800-68-3

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 16800-68-3, name is 1-Acetylindolin-3-one, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C10H9NO2

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 16800-68-3, name is 1-Acetylindolin-3-one, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C10H9NO2

The propyne acid 4 – nitrophenyl-unitz (57.3 mg 0.3 mmol), was used. N- Acetylindole -3 -unitz 26.3 mg (0.15 mmol), the carbene-like (0.015 mmol), 3.96 mg, 1 diazabicycloundecene 8 – (-7 0.3 mmol 45 mul -) and methylene chloride unitunitunito shown in the formula IV are placed in 3 ml a 25 ml unitunito-two-4h port bottle, reacted 30 C, and concentrated, under inert atmosphere protection, unitunitunitaceous conditions, and petroleum ether: petroleum ether: The ethyl acetate ratio 10:1 mixed solvent is eluted, eluent fractions, and the detected eluent fractions of all the products are collected, the solvent is evaporated and 25 mg the solvent is evaporated to obtain the unitz , which is a unitless 75%.

According to the analysis of related databases, 16800-68-3, the application of this compound in the production field has become more and more popular.

Reference:
Patent; China Pharmaceutical University; Du Ding; Sun Kewen; (10 pag.)CN110156800; (2019); A;,
Indoline – Wikipedia,
Indoline | C8H9N – PubChem