The origin of a common compound about 1074-82-4

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 1074-82-4, name is Potassium 1,3-dioxoisoindolin-2-ide, A new synthetic method of this compound is introduced below., Formula: C8H4KNO2

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 1074-82-4, name is Potassium 1,3-dioxoisoindolin-2-ide, A new synthetic method of this compound is introduced below., Formula: C8H4KNO2

Potassium phthalimide (0.93 g; 5.00 mmol), methyl iodide (0.74 g, 5.20 mmol) and DMF (5 mL) were heated at reflux for 1h. The mixture was then poured into water (30 mL) and extracted with dichloromethane (3 × 10 mL). After evaporation of the solvent, the crude product was recrystalized from ethanol.

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Reference:
Article; Zagorski, Piotr M.; Jo?wiak, Andrzej; P?otka, Mieczys?aw W.; Cal, Dariusz; Tetrahedron Letters; vol. 57; 17; (2016); p. 1835 – 1837;,
Indoline – Wikipedia,
Indoline | C8H9N – PubChem