Research on new synthetic routes about 104618-32-8

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 104618-32-8, name is 2-(4-Oxocyclohexyl)isoindoline-1,3-dione, A new synthetic method of this compound is introduced below., Computed Properties of C14H13NO3

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 104618-32-8, name is 2-(4-Oxocyclohexyl)isoindoline-1,3-dione, A new synthetic method of this compound is introduced below., Computed Properties of C14H13NO3

(A) 15gm (0.061 Tmole) 4-phthalimido cyclohexanone was dissolve in 150ml methanol.Heat the mass to 40C. Add Br2 solution (9.8gm Br2 in 25ml of methanol) and 0.25gm ofAids under stirring. Stop stirring and allow initiating bromination and finding clearsolution then add remaining quantity of Br2 solution and stir for 10-15mins. Add 10mlwater and stir for lOmins more. Then filter the white solids obtain .Dry it at 50C for 2-3hrs.YIELD: 12.5gm(62.8%)

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Reference:
Patent; ALEMBIC LIMITED; WO2006/3677; (2006); A1;,
Indoline – Wikipedia,
Indoline | C8H9N – PubChem