Synthetic Route of 4702-13-0, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 4702-13-0, name is N-Phthaloylglycine belongs to indolines-derivatives compound, it is a common compound, a new synthetic route is introduced below.
Phthaloyl glycine (1.0 g, 4.9 mmol) in a 100 mL eggplant-shaped flask was dissolved in dichloromethane (20 mL). Afterwards, oxalyl chloride (2.5 g, 19.6 mmol) and DMF (50 mg) were added. The reaction solution was stirred at room temperature for 30 min and then concentrated. 1.2 g of a pale yellow solid were obtained, which was applied directly to the next step without purification.
The synthetic route of N-Phthaloylglycine has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Yabao Pharmaceutical Group Co., Ltd.; Suzhou Yabao Pharmaceutical Research And Development Co., Ltd.; Song Yang; Qian Xiaoxin; Sun Xiaolin; Li Sailei; Zhu Lin; Zhang Xiyu; Zhang Fei; Wang Peng; (37 pag.)CN109232403; (2019); A;,
Indoline – Wikipedia,
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