Discovery of 3-(1,3-Dioxoisoindolin-2-yl)propanoic acid

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 3339-73-9, name is 3-(1,3-Dioxoisoindolin-2-yl)propanoic acid, A new synthetic method of this compound is introduced below., SDS of cas: 3339-73-9

240 g (1.09 mol) of phthalic anhydride alanine was added to a 1000 mL reaction flask.700 mL of chloroform, warmed to 60 C, and 135 g (1.13 mol) of thionyl chloride was added dropwise.After the completion of the dropwise addition, the reaction was kept for 3 hours, and concentrated under reduced pressure to dryness.Add 400 mL of chloroform to dissolve and set aside.

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Reference:
Patent; Hubei Hongtai Biological Technology Co., Ltd.; Zhang Rui; Lei Yuping; Wang Liming; Wu Weiwei; Li Jianxiong; (8 pag.)CN109053580; (2018); A;,
Indoline – Wikipedia,
Indoline | C8H9N – PubChem