In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 1504-06-9 as follows. SDS of cas: 1504-06-9
To a Schlenk reaction flask with a volume of 20 mL, 0.2 mmol of 3-methyl-2-indanone, 0.4 mmol of morpholine, 0.04 mmol of I2, 0.4 mmol of H 2 O 2 and ethanol (2 mL) were added.The reaction flask was stirred at room temperature under an air atmosphere, and the progress of the reaction was monitored by TLC or GC until the reaction of the starting material was complete (8 hours).The reaction mixture after completion of the reaction was concentrated under reduced pressure, and the residue was purified by column chromatography (ethyl acetate / petroleum ether).
According to the analysis of related databases, 1504-06-9, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Ningbo University; Gao Lehan; Wei Wenting; Bao Wenhui; Xu Xudong; Wang Yining; (10 pag.)CN108440378; (2018); A;,
Indoline – Wikipedia,
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