2913-97-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 2913-97-5, name is N-(2-Oxoethyl)phthalimide belongs to indolines-derivatives compound, it is a common compound, a new synthetic route is introduced below.
To a solution of S-I-Il (6.26 g) and TEA (10.04 g) in dichloromethane (100 mL) at 5-10 ¡ãC was added hydroxylamine hydrochloride (2.53 g). The mixture was stirred at room temperature for 15 h and then quenched with NH4C1(aq) (50 mL, 2M). The aqueous phase was extracted with CH2C12 (2×50 mL). The combined organic NaHCO3(aq)sulfate, filtered. The filtrate was concentrated to get the crude product S-I-Ill (4.01 g, y: 59percent).
The synthetic route of 2913-97-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; NATIONAL HEALTH RESEARCH INSTITUTES; SHIH, Chuan; SHIA, Kak-Shan; WU, Chien-Huang; CHOI, Ming-Chen; SONG, Jen-Shin; WANG, Yun; (84 pag.)WO2018/132326; (2018); A1;,
Indoline – Wikipedia,
Indoline | C8H9N – PubChem